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Beilstein J. Org. Chem. 2019, 15, 840–851, doi:10.3762/bjoc.15.81
Graphical Abstract
Figure 1: Left: Mixed ligand complexes of the type [M2L(μ-L')]n+ supported by the macrocyclic ligand H2L (M =...
Figure 2: Synthesized compounds and their labels.
Scheme 1: Synthesis of complexes 1–9.
Figure 3: 1H NMR spectrum of 6 in CD3CN at 295 K (1.0–8.0 ppm). The resonances and assignments are listed in Table 2...
Figure 4: Structure of the [Zn2L(μ-azo-OH)]+ cation in crystals of [Zn2L(μ-azo-OH)][Zn2L(μ-azo-O)]·4MeCN·3H2O...
Figure 5: Space filling representation of the packing of two symmetry-related [Zn2L(μ-azo-NMe2)]+ cations in ...
Figure 6: Structure of the [Cd2L(μ-azo-NMe2)]+ cation in crystals of [Cd2L(μ-azo-NMe2)]ClO4·0.5MeOH (6·0.5MeO...
Figure 7: Space filling representation of the packing of four [Cd2L(μ-azo-NMe2)]+ cations in crystals of 6·0....
Figure 8: Structures of the two crystallographically independent [Ni2L(μ-azo-NMe2)]+ cations A (left) and B (...
Figure 9: Left: ORTEP representation of the molecular structure of the [Cd2L(μ-azo-CO2Me)]+ cation in crystal...
Figure 10: Plots of the effective magnetic moment μeff for 2 (open circles), 4 (open squares), and 7 (open tri...
Figure 11: UV–vis spectra of Hazo-H (red line), [Cd2L(μ-Cl)](ClO4) (black line) and [Cd2L(μ-azo-H)]ClO4 (1, bl...
Figure 12: UV–vis spectra of Hazo-NMe2 (red line), [Ni2L(μ-Cl)](ClO4) (black line) and [Ni2L(μ-azo-NMe2)]ClO4 (...
Figure 13: UV–vis spectra of solutions of [Cd2L(μ-azo-H)]ClO4 (1) in acetonitrile irradiated with a UV LED lam...
Scheme 2: Cis/trans isomerization process of the bound azo-carboxylato co-ligand in [Cd2L(μ-azo-H)]ClO4 (1) i...